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PRILOGE
Preglednica PI: Ime, okrajšava, navedeni vitamini in njihova vsebnost, oblika, cena za 50 mL in količina izbranih KI.
Št. Ime KI (okrajšava) Navedeni
42
43
44
Preglednica PII: Uporabljena ekstrakcijska topila in njihov volumen pri razvoju ekstrakcijskega postopka.
Sestava V topila [mL]
Topilo 1 MQ 10
Topilo 2 MQ : MeOH = 75 : 25 10
Topilo 3 MQ : MeOH = 50 : 50 10
Topilo 4 MQ : MeOH = 25 : 75 10
Topilo 5 MeOH 10
Topilo 6 HEX : MQ = 2 : 10 12
Topilo 7 HEX : MeOH = 2 : 10 12
Topilo 8 ACN 10
Topilo 9 ACN : MeOH = 50 : 50 10
Topilo 10 ACN : MQ = 50 : 50 10
Slika P1: Kromatogram MQ pri valovni dolžini 210 nm, analiziran po metodi 1.
45
Slika P2: Kromatogram MeOH pri valovni dolžini 260 nm, analiziran po metodi 1.
Slika P3: Kromatogram MeOH pri valovni dolžini 362 nm, analiziran po metodi 2.
46
Slika P4: Kromatogram standarda vitamina B12 pri valovni dolžini 362 nm, analiziran po metodi 2.
Slika P5: Kromatogram standardov vitaminov B6, B3 in B5 (od leve proti desni) pri valovni dolžini 210 nm, analizirani po metodi 1.
47
Slika P6: Kromatogram vitaminov B3 in B5 (od leve proti desni) v vzorcu izdelka BALV pri valovni dolžini 210 nm, analiziran po metodi 1.
Slika P7: Kromatogram vitamina B6 v vzorcu izdelka RB6 pri valovni dolžini 287 nm, analiziran po metodi 1.
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Preglednica PIII: Rezultati vsebnosti vitaminov v izbranih KI in njihova cena za 50 mL.
Ugotovljena vsebnost [% (m/m) ± SD]
Okrajšava
49
Ugotovljena vsebnost [% (m/m) ± SD]
Okrajšava
KI B3 B5 B6 B7 B12
Cena [€/50 mL KI]
LRPHY / 5,005 ± 0,094 / / / 73,4
MABX 1,978 ± 0,080 / / / / 83,2
PCN 11,217 ± 0,257 0,254 ± 0,007 / / / 120
*v KI ga nismo zaznali
Slika P9: Kromatogram standarda vitamina B5 v ACN, analiziran po metodi 1.
Minutes
0,0 0,5 1,0 1,5 2,0 2,5 3,0 3,5 4,0 4,5 5,0 5,5 6,0 6,5 7,0 7,5 8,0
mAU
0 5 10 15 20 25 30 35